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If some small aluminum fluoride species could be solubilized, then perhaps these species could be induced to join together in systematic ways (at low temperatures and in a From a reaction of one-part controlled fashion) to produce new AIF3 phases. trirnethylaluminum with four parts HFopyridine adduct, a precipitate with a formula of [pyridine-H]+oAlF4- is produced in quantitative yield. While this microcrystalline solid is insoluble in most solvents, it was found that it could be rendered soluble by metathesizing the pyridinium cation by slurrying this solid into a solution containing an excess of 1,8bis(dimethylarnino)naphthalene, more commonly known as "proton sponge", PS.
MULTIWAVELENGTH ANOMALOUS-DISPERSION (MAD) PHASING The Physical Basis The ability to choose the wavelength of radiation can be useful in determination of the phase of the diffracted ray, necessary for calculation of the structure. Electrons on heavy atoms, bound to molecules of the specimen, resonate with x-radiation of particular wavelengths. This resonance causes anomalous scattering, in which the diffracted rays have phases and amplitudes that are shifted slightly from rays of different wavelengths.
Figure 10. Left: NADP+ and isocitrate bound to IDH. Right oxalosuccinate (top) and NADPH bound IDH. 34 REFERENCES 1. , and Stanton, M. (1991). Proc. Soc. Photo-Opt. Instr. Eng. 1447, 12-27. 2. , Naday, I. and Westbrook, E. (1993). Proc. Soc. Photo-Opt. Instr. 2009, 133-138. 3. Stanton, M. (1993). Nucl. Instr. and Meth. A325, 550-557. 4. , Naday, I. M. (1993). Nucl. Instr. and Meth. A325, 558-567. 5. Prive, G. and Eisenberg, D. (1995) Personal communication. 6. A. (1994). Crystallographica - A 50, 203-10.